Lab Report Format for Separating the Components of “Panacetin” (2) and Recrystallization and Mellifluous Sharp-end Measurement: Identifying the Components of “Panacetin” (3). Lab Notebook Address and Duration Objective: Elucidate the design of the test and how you artifice to conclude it. Technique: Show the use of separatory funnel and evaporation of solvent setup Reaction(s): Include the main reaction for the test and detachment design Physical Data: List the molecular efficacy, mellifluous sharp-end, effervescence sharp-end, hebetude, solubility, and hazards of all divert chemicals used in the test.
Data/Observations: Your observations of the test, a. Efficacy of judicious panacetin specimen. b. Efficacy of sucrose serene. c. Efficacy of aspirin serene. d. Efficacy of mysterious junction unartificial e. Efficacy of recrystallized mysterious junction f. Mellifluous sharp-end rank of recrystallized mysterious junction. g. TLC sketches delay divert grounds for Rf calculations (Clearly mark each support of spots on the page so I apprehend what it is) h. Mixed mellifluous sharp-end inveterate on notice from TLC Terminal Report ? Address Page.
Include: (1) the address of the test, (2) your spectry, (3) the due duration, and (4) the duration submitted ? Design of the Experiment. ? Background/Setup: ( 1 page) ? Discuss nobility doctrine and elucidate the unconcealed agency of the equipment ? Elucidate the doctrine astern detachment design ? Elucidate the design of recrystillization ? Procedure: relation the process (i. e. passage or handout) and any changes that deviated from the first relation ? Grounds and Results: o Physical description for import(s) unartificial o Efficacy of judicious panacetin specimen. o o o o o o o o o
Weight of sucrose serene. Efficacy of aspirin serene. Efficacy of mysterious junction unartificial Efficacy of recrystallized mysterious junction Mellifluous sharp-end rank of recrystallized mysterious junction. Mixed mellifluous sharp-end inveterate on notice from TLC TLC Cross relation delay lab notebook Rf values from TLC (including the solvent used) Percent resuscitation of sucrose, aspirin and your mysterious ? Calculations: Show specimen calculations of the percent recoveries of sucrose, aspirin and your mysterious and Rf calculations. ? Discussion. What was the unity of your mysterious?
Explain in point how you fixed it, comparing the grounds you obtained delay apprehendn values. Elucidate any discrepancies. (1 page) ? Conclusion: weak announcement delay terminal quittance (restating the end of the lab and summarizing relevant grounds showing that the end was or was not achieved) ? Excercises: Lab 2 questions 1,3,5 Lab 3:1 and 2 Additional Question: Where in the disengagement process could you induce one or further of the Panacetin rudiments? Elucidate which rudiment could be obsolete in which plod. Ignore pursue amounts left in containers, or braying spills.